Single-Domain Nanosphere Observation and Ferromagnetic/Antiferromagnetic Coupling of Ni/NiO
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摘要: 使用微波辅助聚合方法制备了单分散单畴Ni纳米球,由MFM发现,尺度分布在100~180 nm的Ni球的一个相关特征是条型磁畴结构。用XRD、TEM、XPS以及EDAX测量了由Ni球进一步制备的NicoreNiOshell高度球型纳米结构。用VSM 和SQUID进一步讨论了其铁磁/反铁磁界面耦合效应,估算了交换耦合场与粒子尺寸的关系。
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关键词:
- 单分散单畴Ni纳米颗粒 /
- NicoreNiOshell结构 /
- 铁磁/反铁磁界面耦合
Abstract: Magnetic force microscopy (MFM) measurements were performed on monodispersed single-domain nickel nanospheres fabricated by the microwave-assisted (MW) polyol method. As found by MFM, a relevant characteristic of these spheres with a size distribution in the 100~180 nm range is the magnetic stripe domain structure. The obtained highly globular nanostructures of NicoreNiOshell were measured by XRD, TEM, XPS, and EDAX. The ferromagnet/antiferromagnet interface coupling is discussed with the results of VSM and SQUID. The relation of the exchange-coupling field with particles sizes is evaluated. -
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