基于国产铰链式六面顶压机的大腔体静高压技术研究进展

王海阔 贺端威 许超 管俊伟 王文丹 寇自力 彭放

引用本文:
Citation:

基于国产铰链式六面顶压机的大腔体静高压技术研究进展

    通讯作者: 贺端威, duanweihe@scu.edu.cn

Development of Large Volume-High Static Pressure Techniques Based on the Hinge-Type Cubic Presses

    Corresponding author: HE Duan-Wei, duanweihe@scu.edu.cn ;
  • 摘要: 大腔体压机技术因具有静水压性好、样品尺寸大、样品腔内压力与温度分布均匀,且可与同步辐射X射线、中子衍射、超声测量等技术结合对样品进行原位测量等优点,越来越受到高压领域科研工作者的青睐。国内大腔体压机技术多基于国产铰链式六面顶压机构架,国产六面顶压机常规一级压腔所能产生的压力极限较低,约为6 GPa,在一定程度上制约了国内高压科学及相关学科的发展。近几年,基于国产六面顶压机,设计了两种一级压腔增压系统,集成了6-8型二级压腔加压装置。目前,在提供厘米量级样品的前提下,设计的两种一级压腔所能达到的最高压力约为10 GPa;若采用硬质合金二级顶锤,设计的6-8型二级压腔所能达到的最高压力约为20 GPa。最近,自行设计并制备了可产生高于50 GPa压力的多晶金刚石二级顶锤,采用此种顶锤将基于国产六面顶压机构建的二级加压系统的压力标定至35 GPa,拓展了国内大腔体静高压技术的压力产生范围。
  • [1] Irifune T, Kurio A, Sakamoto S, et al. Materials: Ultrahard polycrystalline diamond from graphite [J]. Nature, 2003, 421: 599-600.
    [2] Qin J Q, He D W, Wang J H, et al. Is Rhenium diboride a superhard material? [J]. Adv Mater, 2008, 20(24): 4780-4783.
    [3] Tian Y J, Xu B, Yu D L, et al. Ultrahard nanotwinned cubic boron nitride [J]. Nature, 2013, 493: 385-388.
    [4] Xu C, He D W, Wang H K, et al. Nano-polycrystalline diamond formation under ultra-high pressure [J]. Int J Refract Metals Hard Mater, 2013, 36: 232-237.
    [5] Oganov A R, Ono S. Theoretical and experimental evidence for a post-perovskitephase of MgSiO3 in Earth's D layer [J]. Nature, 2004, 430: 445-448.
    [6] Ma Y M, Eremets M, Oganov A R, et al. Transparent dense sodium [J]. Nature, 2009, 458: 182-185.
    [7] Hemley R J, Soos Z G, Hanfland M, et al. Charge-transfer states in dense hydrogen charge-transfer states in dense hydrogen [J]. Nature, 1994, 369: 384-387.
    [8] Wang H K, He D W, Xu C, et al. Calibration of pressure to 35 GPa for the cubic press using the diamond-cemented carbide compound anvil [J]. Acta Phys Sin, 2013, 62(18): 180703. (in Chinese)
    [9] 王海阔, 贺端威, 许超, 等. 复合型多晶金刚石末级压砧的制备并标定六面顶压机6-8型压腔压力至35 GPa [J]. 物理学报, 2013, 62(18): 180703.
    [10] Dubrovinsky L, Dubrovinskaia N, Prakapenka V B, et al. Implementation of micro-ball nanodiamond anvils for high-pressure studies above 6 Mbar [J]. Nat Commun, 2012, 3: 1163.
    [11] Jayaraman A. Ultrahigh pressures [J]. Rev Sci Instrum, 1986, 57(6): 1013-1031.
    [12] Andrault D, Fiquet G. Synchrotron radiation and laser heating in a diamond anvil cell [J]. Rev Sci Instrum, 2001, 72(2): 1283-1288.
    [13] Klotz S, Besson J M, Hamel G, et al. Neutron powder diffraction at pressures beyond 25 GPa [J]. Appl Phys Lett, 1995, 66(14): 1735-1737.
    [14] Fan D W, Wei S Y, Xie H S. An in situ high-pressure X-ray diffraction experiment on hydroxyapophyllite [J]. Chinese Physics B, 2013, 22: 010702.
    [15] Sung C M. A century of progress in the development of very high pressure apparatus for scientific research and diamond synthesis [J]. High Temp-High Press, 1997, 29: 253-293.
    [16] He D W, Wang H K, Tan N, et al. An anvil-preformed gasket apparatus: China, 201010142804. 7 [P]. 2010-08-18. (in Chinese)
    [17] 贺端威, 王海阔, 谭宁, 等. 一种顶锤-预密封边高压装置: 中国, 201010142804. 7 [P]. 2010-08-18.
    [18] Wang H K, He D W. A new large-volume high pressure apparatus: China, 201110091480. 3 [P]. 2011-09-21. (in Chinese)
    [19] 王海阔, 贺端威. 一种新型大腔体高压装置: 中国, 201110091480. 3 [P]. 2011-09-21.
    [20] Li Z C, Jia X P, Huang G F, et al. FEM simulations and experimental studies of the temperature field in a large diamond crystal growth cell [J]. Chinese Physics B, 2013, 22: 014701.
    [21] Yu G, Han Q G, Li M Z, et al. Finite element analysis of the high-pressure tungsten carbide radius-anvil [J]. Acta Phys Sin, 2012, 61: 040702. ( in Chinese)
    [22] 于歌, 韩奇钢, 李明哲, 等. 新型圆角式高压碳化钨硬质合金顶锤的有限元分析 [J]. 物理学报, 2012, 61: 040702.
    [23] Khvostantsev L G. A verkh-niz (up-down) toroid device for generation of high pressure [J]. High Temp-High Pressure, 1984, 16: 165-169.
    [24] Wang H K. Development and application of pressure generation techniques based on hinge-type cubic press [D]. Chengdu: Institute of Atomic and Molecular Physics, Sichuan University, 2008: 8-13. (in Chinese)
    [25] 王海阔. 基于国产六面顶压机增压装置的压力产生极限扩展与应用 [D]. 成都: 四川大学原子分子物理研究所, 2008: 8-13.
    [26] Wang H K, He D W, Tan N, et al. An anvil-preformed gasket system to extend the pressure range for large volume cubic presses [J]. Rev Sci Instrum, 2010, 81: 116101.
    [27] Wang H K, He D W, Yan X Z, et al. Quantitative measurements of pressure gradients for the pyrophyllite and magnesium oxide pressure-transmitting mediums to 8 GPa in a large-volume cubic cell [J]. High Press Res, 2011, 31: 581-591.
    [28] Wang H K, He D W. A hybrid pressure cell of pyrophyllite and magnesium oxide to extend the pressure range for large volume cubic presses [J]. High Press Res, 2012, 32: 186-194.
    [29] Liebermann Robert C, Wang Y B. High-Pressure Research: Application to Earth and Planetary Sciences [M]. Washington DC: AGU. 1992: 19.
    [30] Tange Y, Irifune T, Funakoshi K, et al. Pressure generation to 80 GPa using multianvil apparatus with sintered diamond anvils [J]. High Press Res, 2008, 28: 245-254.
    [31] Kunimoto T, Irifune T. Pressure generation to 125 GPa using a 6-8-2 type multianvil apparatus with nano-polycrystalline diamond anvils [J]. J Phys: Conf Ser, 2010, 215: 02190.
    [32] Wang F L, He D W, Fang L M, et al. Design and assembly of split-sphere high pressure apparatus based on the hinge-type cubic-anvil press [J]. Acta Phys Sin, 2008, 57: 5429-5434. (in Chinese)
    [33] 王福龙, 贺端威, 房雷鸣, 等. 基于铰链式六面顶压机的二级6-8型大腔体静高压装置 [J]. 物理学报, 2008, 57: 5429-5434.
    [34] Wang W D, He D W, Wang H K, et al. Reaserch on pressure generation efficiency of 6-8 type multianvil high pressure apparatus [J]. Acta Phys Sin, 2010, 59: 3107. (in Chinese)
    [35] 王文丹, 贺端威, 王海阔, 等. 二级6-8型大腔体装置的高压发生效率机理研究 [J]. 物理学报, 2010, 59: 3107-3115.
    [36] Guan J W, He D W, Wang H K, et al. Influence of mechanical configuration and hardness of last stage anvil on high pressure producing efficiency for octahedral cell [J]. Acta Phys Sin, 2012, 61: 100701. (in Chinese)
    [37] 管俊伟, 贺端威, 王海阔, 等. 力学结构及末级压砧硬度对八面体压腔高压发生效率的影响 [J]. 物理学报, 2012, 61: 100701.
    [38] Daniels W B, Jones M T. Simple apparatus for the generation of pressures above 100000 atmospheres simultaneously with temperatures above 3000 ℃ [J]. Rev Sci Instrum, 1961, 32: 885-888.
    [39] Xi L, Chen J L, Tang J J, et al. A large volume cubic press with a pressure-generating capability up to about 10 GPa [J]. High Press Res, 2012, 32: 239-254.
    [40] Fang L M, He D W, Chen C, et al. Effect of precompression on pressure-transmitting efficiency of pyrophyllite gaskets [J]. High Press Res, 2007, 27: 367-374.
    [41] Andersson G, Sundqvist B, Backstrom G. A high-pressure cell for electrical resistance measurements at hydrostatic pressures up to 8 GPa: Results for Bi, Ba, and Si [J]. J Appl Phys, 1989, 65(10): 3943.
    [42] Ma H A, Jia X P, Chen L X, et al. High-pressure pyrolysis study of C3N6H6: A route to preparing bulk C3N4 [J]. J Phys Condens Matter, 2002, 14: 11269-11273.
    [43] Wentorff R H, Bundy F P. Modern Very High Pressure Techniques [M]. London: Butterworths, 1962: 1-24.
    [44] Duffy T S, Hemley R J, Mao H K. Equation of state and shear strength at multimegabar pressures: Magnesium oxide to 227 GPa [J]. Phys Rev Lett, 1995, 74: 1371-1374.
    [45] Perez-Albuerne E A, Drickamer H G. Effect of high pressures on the compressibilities of seven crystals having the NaCl or CsCl structure [J]. J Chem Phys, 1965, 43: 1381-1386.
    [46] Lloyd E C. Accurate Characterization of the High Pressure Environment: Proceedings of a Symposium Held at the National Bureau of Standards [M]. Washington, DC: NBS Special Publication, 1971: 189.
    [47] Mao H K, Bell P M. Equations of state of MgO and -Fe under static pressure conditions [J]. J Geophys Res, 1979, 84: 4533-4536.
    [48] Wang H K. Development and application of pressure generation techniques based on hinge-type cubic press [D]. Chengdu: Institute of Atomic and Molecular Physics, Sichuan University, 2008: 14. (in Chinese)
    [49] 王海阔. 基于国产六面顶压机增压装置的压力产生极限扩展与应用 [D]. 成都: 四川大学原子分子物理研究所, 2008: 14.
    [50] Wang H K. Development and application of pressure generation techniques based on hinge-type cubic press [D]. Chengdu: Institute of Atomic and Molecular Physics, Sichuan University, 2008: 87-109. (in Chinese)
    [51] 王海阔. 基于国产六面顶压机增压装置的压力产生极限扩展与应用 [D]. 成都: 四川大学原子分子物理研究所, 2008: 87-109.
    [52] L S J, Luo J T, Shu L, et al. A slide-type multianvil ultrahigh pressure apparatus and calibrations of its pressure and temperature [J]. Acta Phys Sin, 2009, 58: 6852-6857. (in Chinese)
    [53] 吕世杰, 罗建太, 苏磊, 等. 滑块式六含八超高压实验装置及其压力温度标定 [J]. 物理学报, 2009, 58: 6852-6857.
    [54] Frost D J, Poe B T, Trnnes R G, et al. A new large-volume multianvil system [J]. Phys Earth Planet Int, 2004, 143-144: 507-514.
    [55] Getting I C. New determination of the bismuth Ⅰ-Ⅱ equilibrium pressure: A proposed modification to the practical pressure scale [J]. Metrologia, 998, 35: 119.
    [56] Lloyd E C. Accurate Characterization of the High-pressure Environment: Proceedings of a Symposium Held at the National Bureau of Standards [M]. Washington, DC: NBS Special Publication, 1971: 326.
    [57] Ohtani A, Motobayashi M, Onodera A. Polymorphism of ZnTe at elevated pressure [J] . Phys Lett A, 1980, 75: 435-437.
    [58] Ovsyannikov S V, Shchennikov V V. Application of the high-pressure thermoelectric technique for characterization of semiconductor microsamples: PbX-based compounds [J]. Solid State Commun, 2004, 37: 1151.
    [59] Jiang J Z, Gerward L, Frost D, et al. Grain-size effect on pressure-induced semiconductor-to-metal transition in ZnS [J]. J Appl Phys, 1999, 86: 6608-6610.
    [60] Yagi T, Akimoto S. Direct determination of coesite-stishovite transition by in-situ X-ray measurements [J]. J Appl Phys, 1976, 47: 259-270.
    [61] Xu C, He D W, Wang H K, et al. Synthesis of nano-polycrystalline diamond under high pressure and high temperature [J]. Superhard Material Engineering, 2011, 4: 001-003. (in Chinese)
    [62] 许超, 贺端威, 王海阔, 等. 纳米聚晶金刚石的高压高温合成 [J]. 超硬材料工程, 2011, 4: 001-003.
    [63] Kawazoe T, Nishiyama N, Nishihara Y, et al. Pressure generation to 25 GPa using a cubic anvil apparatus with a multi-anvil 6-6 assembly [J]. High Press Res, 2010, 30: 167-174.
    [64] Wang H K, He D W, Xu C, et al. Nanostructured diamond-TiC composites with high fracture toughness [J]. J Appl Phys, 2013, 113: 043505.
    [65] Wang H K. Development and application of pressure generation techniques based on hinge-type cubic press [D]. Chengdu: Institute of Atomic and Molecular Physics, Sichuan University, 2008: 113-129. (in Chinese)
    [66] 王海阔. 基于国产六面顶压机增压装置的压力产生极限扩展与应用 [D]. 成都: 四川大学原子分子物理研究所, 2008: 113-129.
    [67] Lorenzana H E, Boppart H, Silvera I F. Study of pressure distributions in a megabar diamond indentor cell [J]. Rev Sci Instrum, 1988, 59: 2583-2591.
    [68] Tange Y, Takahashi E, Funakoshi K. In situ observation of pressure-induced electrical resistance changes in zirconium: Pressure calibration points for the large volume press at 8 and 35 GPa [J]. High Press Res, 2011, 31: 413-418.
    [69] Wang H K. Development and application of pressure generation techniques based on hinge-type cubic press [D]. Chengdu: Institute of Atomic and Molecular Physics, Sichuan University, 2008: 131-140. (in Chinese)
    [70] 王海阔. 基于国产六面顶压机增压装置的压力产生极限扩展与应用 [D]. 成都: 四川大学原子分子物理研究所, 2008: 131-140.
    [71] Wang H K. Development and application of pressure generation techniques based on hinge-type cubic press [D]. Chengdu: Institute of Atomic and Molecular Physics, Sichuan University, 2008: 63-84. (in Chinese)
    [72] 王海阔. 基于国产六面顶压机增压装置的压力产生极限扩展与应用 [D]. 成都: 四川大学原子分子物理研究所, 2008: 63-84.
  • [1] 陈晓芳贺端威王福龙张剑李拥军房雷鸣雷力寇自力 . 基于铰链式六面顶压机的二级6-8模超高压大腔体内置加热元件的设计与温度标定. 高压物理学报, 2009, 23(2): 98-104 . doi: 10.11858/gywlxb.2009.02.004
    [2] 杨宗庆吴兆庆王伟东张友俊李嘉 . 合成金刚石超高压腔内的压力剃度. 高压物理学报, 1987, 1(2): 176-183 . doi: 10.11858/gywlxb.1987.02.012
    [3] 孙悦毕延董越罗湘捷丁立业杨向东 . 六面顶压机集中控制系统的组态设计. 高压物理学报, 2003, 17(3): 235-240 . doi: 10.11858/gywlxb.2003.03.014
    [4] 张佳威李强王俊普贺端威 . 二次加压对六面顶压腔压力发生效率和压力密封性能的影响. 高压物理学报, 2019, 33(2): 020105-1-020105-8. doi: 10.11858/gywlxb.20190703
    [5] 彭放贺端威 . 应用于高压科学研究的国产铰链式六面顶压机技术发展历程. 高压物理学报, 2018, 32(1): 010105-1-010105-6. doi: 10.11858/gywlxb.20170600
    [6] 王永坤贺端威陈宏洋王文丹刘方明何飞张瑜胡艺寇自力彭放高上攀马迎功杨兴辉 . 利用围压提高二级大腔体静高压装置压力极限的初步实验探索. 高压物理学报, 2015, 29(3): 223-231. doi: 10.11858/gywlxb.2015.03.010
    [7] 张聪马红安韩奇钢李战厂贾晓鹏 . 高压下国产六面顶压机铰链梁和工作缸的应力分析. 高压物理学报, 2010, 24(5): 321-325 . doi: 10.11858/gywlxb.2010.05.001
    [8] 于川庞勇曹仁义虞德水孙永强张蓉杨桂红仝延锦施尚春朱子标张旭 . 小型车载式二级轻气炮加载系统的爆轰实验研究. 高压物理学报, 2013, 27(5): 763-767. doi: 10.11858/gywlxb.2013.05.017
    [9] 邓云飞张伟贾斌庞宝君曹宗胜 . 二级轻气炮遮挡式激光光幕测速系统. 高压物理学报, 2011, 25(4): 296-302 . doi: 10.11858/gywlxb.2011.04.002
    [10] 刘巍杜建国于泳白利平王传远 . 六面顶压机高温高压弹性波速测量装置样品室温度梯度的校正. 高压物理学报, 2003, 17(2): 95-100 . doi: 10.11858/gywlxb.2003.02.003
    [11] 何强唐俊杰王霏刘曦 . 一种适用于极端高温条件的六面顶压机实验组装. 高压物理学报, 2014, 28(2): 145-151. doi: 10.11858/gywlxb.2014.02.003
    [12] 孙珠妹胡栋施尚春沈寿彭 . 聚偏氟乙烯对高速气流的响应二级轻气炮分流系统特性的测量. 高压物理学报, 1991, 5(3): 233-240 . doi: 10.11858/gywlxb.1991.03.012
    [13] 王翔王为傅秋卫 . 用于一级轻气炮的弹速激光测量系统. 高压物理学报, 2003, 17(1): 75-80 . doi: 10.11858/gywlxb.2003.01.012
    [14] 罗斌强赵剑衡孙承纬莫建军贺佳张兴卫王桂吉谭福利 . 二级电炮加载技术研究. 高压物理学报, 2012, 26(3): 251-258. doi: 10.11858/gywlxb.2012.03.002
    [15] 陆中战晓红曹大呼张良莹姚熹 . 一套基于六面顶高压装置的静水压高频介电测试系统. 高压物理学报, 2008, 22(1): 99-102 . doi: 10.11858/gywlxb.2008.01.021
    [16] 吴静蓝强王青松鲜海峰贾路峰傅秋卫 . 二级轻气炮压缩级发射技术研究. 高压物理学报, 2006, 20(4): 445-448 . doi: 10.11858/gywlxb.2006.04.018
    [17] 郑海飞孙樯赵金段体玉 . 金刚石压腔高温高压实验的压力标定方法及其现状. 高压物理学报, 2004, 18(1): 78-82 . doi: 10.11858/gywlxb.2004.01.014
    [18] 何飞贺端威马迎功晏小智刘方明王永坤刘进寇自力彭放 . 二级6-8型静高压装置厘米级腔体的设计原理与实验研究. 高压物理学报, 2015, 29(3): 161-168. doi: 10.11858/gywlxb.2015.03.001
    [19] 赵士操宋振飞姬广富龚自正赵晓平 . 一种基于二级轻气炮平台的超高速弹丸发射装置设计. 高压物理学报, 2011, 25(6): 557-564. doi: 10.11858/gywlxb.2011.06.012
    [20] 文尚刚孙承纬赵锋谭多望 . 平面二级炸药强爆轰驱动装置的优化设计. 高压物理学报, 2009, 23(2): 81-86 . doi: 10.11858/gywlxb.2009.02.001
  • 加载中
计量
  • 文章访问数:  3780
  • 阅读全文浏览量:  152
  • PDF下载量:  1502
出版历程
  • 收稿日期:  2013-08-27
  • 录用日期:  2013-09-24
  • 刊出日期:  2013-10-15

基于国产铰链式六面顶压机的大腔体静高压技术研究进展

    通讯作者: 贺端威, duanweihe@scu.edu.cn
  • 1. 四川大学原子与分子物理研究所,四川成都 610065;
  • 2. 河南工业大学材料科学与工程学院,河南郑州 450001

摘要: 大腔体压机技术因具有静水压性好、样品尺寸大、样品腔内压力与温度分布均匀,且可与同步辐射X射线、中子衍射、超声测量等技术结合对样品进行原位测量等优点,越来越受到高压领域科研工作者的青睐。国内大腔体压机技术多基于国产铰链式六面顶压机构架,国产六面顶压机常规一级压腔所能产生的压力极限较低,约为6 GPa,在一定程度上制约了国内高压科学及相关学科的发展。近几年,基于国产六面顶压机,设计了两种一级压腔增压系统,集成了6-8型二级压腔加压装置。目前,在提供厘米量级样品的前提下,设计的两种一级压腔所能达到的最高压力约为10 GPa;若采用硬质合金二级顶锤,设计的6-8型二级压腔所能达到的最高压力约为20 GPa。最近,自行设计并制备了可产生高于50 GPa压力的多晶金刚石二级顶锤,采用此种顶锤将基于国产六面顶压机构建的二级加压系统的压力标定至35 GPa,拓展了国内大腔体静高压技术的压力产生范围。

English Abstract

参考文献 (72)

目录

    /

    返回文章
    返回