Design and Experimental Research of the Graphite Heating Assembly of Centimeter-Size Chamber for Two-Stage 6-8 Type Multi-Anvil High Pressure Apparatus

WANG Qiang; HE Duan-Wei; LIU Jin; LIU Fang-Ming; DING Wei; MA Ying-Gong; LIU Teng; LI Yuan-Yuan; WU Jing-Jun; ZHANG Jia-Wei; KOU Zi-Li

doi:10.11858/gywlxb.2017.05.002

Volume 31 Issue 5

Nov 2017

Turn off MathJax

Article Contents

Chinese Journal of High Pressure Physics > 2017 > 31(5): 511-520.

WANG Qiang, HE Duan-Wei, LIU Jin, LIU Fang-Ming, DING Wei, MA Ying-Gong, LIU Teng, LI Yuan-Yuan, WU Jing-Jun, ZHANG Jia-Wei, KOU Zi-Li. Design and Experimental Research of the Graphite Heating Assembly of Centimeter-Size Chamber for Two-Stage 6-8 Type Multi-Anvil High Pressure Apparatus[J]. Chinese Journal of High Pressure Physics, 2017, 31(5): 511-520. doi: 10.11858/gywlxb.2017.05.002

Citation:

WANG Qiang, HE Duan-Wei, LIU Jin, LIU Fang-Ming, DING Wei, MA Ying-Gong, LIU Teng, LI Yuan-Yuan, WU Jing-Jun, ZHANG Jia-Wei, KOU Zi-Li. Design and Experimental Research of the Graphite Heating Assembly of Centimeter-Size Chamber for Two-Stage 6-8 Type Multi-Anvil High Pressure Apparatus[J]. Chinese Journal of High Pressure Physics, 2017, 31(5): 511-520. doi: 10.11858/gywlxb.2017.05.002

Citation:

WANG Qiang, HE Duan-Wei, LIU Jin, LIU Fang-Ming, DING Wei, MA Ying-Gong, LIU Teng, LI Yuan-Yuan, WU Jing-Jun, ZHANG Jia-Wei, KOU Zi-Li. Design and Experimental Research of the Graphite Heating Assembly of Centimeter-Size Chamber for Two-Stage 6-8 Type Multi-Anvil High Pressure Apparatus[J]. Chinese Journal of High Pressure Physics, 2017, 31(5): 511-520. doi: 10.11858/gywlxb.2017.05.002

PDF( 5403 KB)

Design and Experimental Research of the Graphite Heating Assembly of Centimeter-Size Chamber for Two-Stage 6-8 Type Multi-Anvil High Pressure Apparatus

doi: 10.11858/gywlxb.2017.05.002

WANG Qiang^{1, 2
,},
HE Duan-Wei^{1, 2,*
,
,},
LIU Jin^{1, 2},
LIU Fang-Ming^{1, 2},
DING Wei^{1, 2},
MA Ying-Gong^{1, 2},
LIU Teng^{1, 2},
LI Yuan-Yuan^{1, 2, 3},
WU Jing-Jun^{1, 2},
ZHANG Jia-Wei^{1, 2},
KOU Zi-Li¹

1.
Institute of Atomic and Molecular Physics, Sichuan University, Chengdu 610065, China
2.
Key Laboratory of High Energy Density Physics and Technology of Ministry of Education, Sichuan University, Chengdu 610065, China
3.
Institute of Fluid Physics, CAEP, Mianyang 621999, China

Received Date: 12 Mar 2017
Rev Recd Date: 13 Apr 2017

Abstract

Abstract

We designed a built-in graphite heating assembly, called "Bridge", based on a domestic 6-8 type static high pressure apparatus and using the cut-apex three-segment 36/20 assembly, and obtained the relationship between the heating power and the temperature using the high pressure in-situ measurement technology.We also achieved a stable p-T (2.5-10.4 GPa; 0-1 650/1 800 ℃) region.Moreover, we successfully synthesized a centimeter sample under high pressure and at high temperature, one that can reach 13 mm.We discussed the relation between the resistances of the assembly and the heating temperature, and analyzed the cause of the resistance change.The temperature distribution of the assemble was reflected by the characterization of the sample.This study will broaden the applicability of the domestic hinge-type cubic-anvil press 6-8 type static high pressure apparatus, and offer a better practicability.

FullText(HTML)

References(31)

References

[1]	IRIFUNE T, KURIO A, SAKAMOTO S, et al.Materials:ultrahard polycrystalline diamond from graphite[J].Nature, 2003, 421(6923):599-600. http://d.old.wanfangdata.com.cn/Periodical/cuihuaxb201601001
[2]	TIAN Y, XU B, YU D, et al.Ultrahard nanotwinned cubic boron nitride[J].Nature, 2013, 493(7432):385-388. doi: 10.1038/nature11728
[3]	WANG S, HE D, WANG W, et al.Pressure calibration for the cubic press by differential thermal analysis and the high-pressure fusion curve of aluminum[J].High Pressure Res, 2009, 29(4):806-814. doi: 10.1080/08957950903335521
[4]	赵有祥, 徐小平, 陈红, 等.环状容器内的温度校正和高压下温度相关性问题[J].物理学报, 1979, 28(6):872-876. doi: 10.3321/j.issn:1000-3290.1979.06.013 ZHAO Y X, XU X P, CHEN H, et al.Temperature measurement in "belt" apparatus and problem of temperature correlation at high pressures [J].Acta Phys Sin, 1979, 28(6):872-876. doi: 10.3321/j.issn:1000-3290.1979.06.013
[5]	王海阔, 贺端威, 许超, 等.基于国产铰链式六面顶压机的大腔体静高压技术研究进展[J].高压物理学报, 2013, 27(5):633-661. http://www.gywlxb.cn/CN/abstract/abstract1618.shtml WANG H K, HE D W, XU C, et al.Development of large volume-high static pressure techniques based on the hinge-type cubic presses[J].Chinese Journal of High Pressure Physics, 2013, 27(5):633-661. http://www.gywlxb.cn/CN/abstract/abstract1618.shtml
[6]	亓曾笃.人造金刚石生长中的温度控制[J].高压物理学报, 1990, 4(3):204-209. http://www.gywlxb.cn/CN/abstract/abstract1618.shtml QI Z D.The temperature control for the crowth of sythetic diamond[J].Chinese Journal of High Pressure Physics, 1990, 4(3):204-209. http://www.gywlxb.cn/CN/abstract/abstract1618.shtml
[7]	XIE L, YONEDA A, YOSHINO T, et al.Graphite-boron composite heater in a Kawai-type apparatus:the inhibitory effect of boron oxide and countermeasures[J].High Pressure Res, 2016, 36(2):105-120. doi: 10.1080/08957959.2016.1164151
[8]	SHATSKIY A, KATSURA T, LITASOV K D, et al.High pressure generation using scaled-up Kawai-cell[J].Phys Earth Planet Inter, 2011, 189(1/2):92-108. http://d.old.wanfangdata.com.cn/NSTLQK/NSTL_QKJJ0224900744/
[9]	方啸虎, 温简杰, 郑日升.中国超硬材料新态势[J].超硬材料工程, 2010, 22(1):18-21. doi: 10.3969/j.issn.1673-1433.2010.01.004 FANG X H, WEN J J, ZHENG R S, et al.New trends of china superhard materials[J].Superhard Material Engineering, 2010, 22(1):18-21. doi: 10.3969/j.issn.1673-1433.2010.01.004
[10]	贾晓鹏.优质Ⅱa型宝石级金刚石的合成技术[J].金刚石与磨料磨具工程, 2005(3):8-11. doi: 10.3969/j.issn.1006-852X.2005.03.002 JIA X P.Technology of growing large crystals of high quality type-Ⅱ a diamond crystal[J].Diamond & Abrasives Engineering, 2005(3):8-11. doi: 10.3969/j.issn.1006-852X.2005.03.002
[11]	何强, 唐俊杰, 王霏, 等.一种适用于极端高温条件的六面顶压机实验组装[J].高压物理学报, 2013, 28(2):145-151. http://www.gywlxb.cn/CN/abstract/abstract1618.shtml HE Q, TANG J J, WANG F, et al.High temperature stable assembly designed for cubic press [J].Chinese Journal of High Pressure Physics, 2013, 28(2):145-151. http://www.gywlxb.cn/CN/abstract/abstract1618.shtml
[12]	杜建国, 贺端威, 高春晓, 等.矿物岩石高温高压实验与理论研究[M].北京:地震出版社, 2011:8-11. DU J G, HE D W, GAO C X, et al.Experimental and theoretical studies of mineral and rock at high pressure and temperature [M].Beijing:Earthquake Press, 2011:8-11
[13]	王文丹, 贺端威, 王海阔, 等.二级6-8型大腔体装置的高压发生效率机理研究[J].物理学报, 2010, 59(5):3107-3115. http://d.old.wanfangdata.com.cn/Periodical/wlxb201005030 WANG W D, HE D W, WANG H K, et al.Research on pressure generation efficiency of 6-8 type multi-anvil high pressure apparatus [J].Acta Phys Sin, 2010, 59(5):3107-3015. http://d.old.wanfangdata.com.cn/Periodical/wlxb201005030
[14]	XU C, HE D, WANG H, et al.Nano-polycrystalline diamond formation under ultra-high pressure[J].Int J Refract Metals Hard Mater, 2013, 36(1):232-237. http://d.old.wanfangdata.com.cn/NSTLQK/NSTL_QKJJ0229996906/
[15]	何飞, 贺端威, 马迎功, 等.二级6-8型静高压装置厘米级腔体的设计原理与实验研究[J].高压物理学报, 2015, 29(3):161-168. http://www.gywlxb.cn/CN/abstract/abstract1799.shtml HE F, HE D W, MA Y G, et al.Design principles and experimental study of centimeter-scale sample chamber for two-stage 6-8 type static high pressure apparatus[J].Chinese Journal of High Pressure Physics, 2015, 29(3):161-168. http://www.gywlxb.cn/CN/abstract/abstract1799.shtml
[16]	马迎功, 贺端威, 韩晶晶, 等.二级6-8型静高压装置厘米级腔体内置加热元件的设计与温度标定[J].高压物理学报, 2017, 31(1):61-66. http://www.gywlxb.cn/CN/abstract/abstract1930.shtml MA Y G, HE D W, HAN J J, et al.Design and temperature calibration for heater cell of centimeter-scale sample chamber for two-stage 6-8 type static high pressure apparatus[J].Chinese Journal of High Pressure Physics, 2017, 31(1):61-66. http://www.gywlxb.cn/CN/abstract/abstract1930.shtml
[17]	陈晓芳, 贺端威, 王福龙, 等.基于铰链式六面顶压机的二级6-8模超高压大腔体内置加热元件的设计与温度标定[J].高压物理学报, 2009, 23(2):98-104. doi: 10.3969/j.issn.1000-5773.2009.02.004 CHEN X F, HE D W, WANG F L, et al.Split-sphere high pressure apparatus based on hinge-type cubic-anvil press [J].Chinese Journal of High Pressure Physics, 2009, 23(2):98-104. doi: 10.3969/j.issn.1000-5773.2009.02.004
[18]	吕世杰, 罗建太, 苏磊, 等.滑块式六含八超高压实验装置及其压力温度标定[J].物理学报, 2009, 58(10):6852-6857. http://d.old.wanfangdata.com.cn/Periodical/wlxb200910031 LV S J, LUO J T, SU L, et al.A slide-type multianvil ultrahigh pressure apparatus and calibration of its pressure and temperature[J].Acta Phys Sin, 2009, 58(10):6852-6857. http://d.old.wanfangdata.com.cn/Periodical/wlxb200910031
[19]	亓曾笃.金刚石生产的加热方法[J].超硬材料与宝石, 2002, 14(4):26-28. http://d.old.wanfangdata.com.cn/Periodical/zbkj200204008 QI Z D.The heating mathods of diamond production[J].Superhard Material & GEM, 2002, 14(4):26-28. http://d.old.wanfangdata.com.cn/Periodical/zbkj200204008
[20]	HERNLUND J.A numerical model for steady-state temperature distributions in solid-medium high-pressure cell assemblies[J].Am Mineralog, 2006, 91(2/3):295-305.
[21]	方啸虎, 邓福铭, 郑日升.现代超硬材料与制品[M].杭州:浙江大学出版社, 2011:181-189. FANG X H, DENG F M, ZHENG R S, et al.Adanced superabrasives and related products[M].Hangzhou:Zhejiang University Press, 2011:181-189.
[22]	郭欣, 刘衍聪, 伊鹏.六面顶压机合成金刚石加热规律研究[J].人工晶体学报, 2010, 39(4):966-971. doi: 10.3969/j.issn.1000-985X.2010.04.028 GUO X, LIU Y C, YI P.Study on the law of heating process of diamond synthesized by cubic anvil press[J].Journal of High Synthetic Crystals, 2010, 39(4):966-971. doi: 10.3969/j.issn.1000-985X.2010.04.028
[23]	冯吉福, 林峰, 李立惟, 等.六面顶压机上不同组装结构的温度研究[J].超硬材料工程, 2009, 21(3):21-25. doi: 10.3969/j.issn.1673-1433.2009.03.005 FENG J F, LIN F, LI L W, et al.Study on temperature of different assembly structure in cubic hinge apparatus[J].Superhard Material Engineering, 2009, 21(3):21-25. doi: 10.3969/j.issn.1673-1433.2009.03.005
[24]	杨君刚.材料加热炉基础[M].西安:西北工业大学出版社, 2009:134-137. YANG J G.Material heating furnace foundation[M].Xi'an:Northwestern Industry University Press, 2009:134-137.
[25]	王秦生.超硬材料及制品[M].郑州:郑州大学出版社, 2006:116-118. WANG Q S.Superhard materials and products [M].Zhengzhou:Zhengzhou University Press, 2006:116-118.
[26]	LIU Y, HE D, LEI L, et al.High pressure infiltration sintering of cBN-Si composites[J].Int J Refract Metals Hard Mater, 2015, 50:247-252. doi: 10.1016/j.ijrmhm.2015.01.006
[27]	LIU G, KOU Z, YAN X, et al.Submicron cubic boron nitride as hard as diamond[J].Appl Phys Lett, 2015, 106(12):121901. doi: 10.1063/1.4915253
[28]	FUJISAKI K, YOKOTA H, FURUSHIRO N, et al.Development of ultra-fine-grain binderless cBN tool for precision cutting of ferrous materials[J].J Mater Proc Technol, 2009, 209(15/16):5646-5652. http://www.wanfangdata.com.cn/details/detail.do?_type=perio&id=c325829517e40df5b37d1dfc8b69ffc3
[29]	刘芳, 刘永刚, 谢鸿森.六面顶压机高压腔体温度场的数值模拟[J].高压物理学报, 2010, 26(2):135-140. http://www.gywlxb.cn/CN/abstract/abstract1437.shtml LIU F, LIU Y G, XIE H S, et al.Numerical simulation of temperature field in sample assembly od cubic press[J].Chinese Journal of High Pressure Physics, 2010, 26(2):135-140. http://www.gywlxb.cn/CN/abstract/abstract1437.shtml
[30]	李瑞, 马红安, 韩奇钢, 等.基于ANSYS的金刚石合成腔内的温度场分析[J].吉林大学学报(工学版), 2008, 38(3):535-538. http://d.old.wanfangdata.com.cn/Periodical/jlgydxzrkxxb200803008 LI R, MA H A, HAN Q G, et al.Analysis of temperature field in diamond synthetic chamber based on ANSYS[J].Journal of Jilin University (Engineering and Technology Edition), 2008, 38(3):535-538. http://d.old.wanfangdata.com.cn/Periodical/jlgydxzrkxxb200803008
[31]	WANG H, HE D, YAN X, et al.Quantitative measurements of pressure gradients for the pyrophyllite and magnesium oxide pressure-transmitting mediums to 8 GPa in a large-volume cubic cell[J].High Pressure Res, 2011, 31(4):581-591. doi: 10.1080/08957959.2011.614238

Relative Articles

Supplements(0)

Cited By

Proportional views

Proportional views

通讯作者: 陈斌, bchen63@163.com

1.
沈阳化工大学材料科学与工程学院沈阳 110142

Figures(13)

Get Citation

PDF

XML

Article Metrics

Article views(7261) PDF downloads(204)

Design and Experimental Research of the Graphite Heating Assembly of Centimeter-Size Chamber for Two-Stage 6-8 Type Multi-Anvil High Pressure Apparatus

doi: 10.11858/gywlxb.2017.05.002

Abstract

References

Proportional views

Catalog

通讯作者: 陈斌, bchen63@163.com

Article Metrics

Proportional views

Related

Design and Experimental Research of the Graphite Heating Assembly of Centimeter-Size Chamber for Two-Stage 6-8 Type Multi-Anvil High Pressure Apparatus

doi: 10.11858/gywlxb.2017.05.002

Abstract

References

Proportional views

Catalog

通讯作者: 陈斌, bchen63@163.com

Article Metrics

Proportional views

Related

Export File

Citation

Format

Content