knowledge of professional and technical personnel Notice on the organization of advanced research class on high-pressure science and new materials of engineering
Volume 24 Issue 3
Apr 2015
Turn off MathJax
Article Contents
Chinese Journal of High Pressure Physics  > 2010  >  24(3): 206-212 .
ZHANG Yi, BI Yan, CAI Ling-Cang, XU Ji-An. Ultrasonic Velocity Measurement and Pressure Calibration of Single Crystal MgO under Hydrostatic Pressure Load[J]. Chinese Journal of High Pressure Physics, 2010, 24(3): 206-212 . doi: 10.11858/gywlxb.2010.03.008
Citation: ZHANG Yi, BI Yan, CAI Ling-Cang, XU Ji-An. Ultrasonic Velocity Measurement and Pressure Calibration of Single Crystal MgO under Hydrostatic Pressure Load[J]. Chinese Journal of High Pressure Physics, 2010, 24(3): 206-212 . doi: 10.11858/gywlxb.2010.03.008
shu

Ultrasonic Velocity Measurement and Pressure Calibration of Single Crystal MgO under Hydrostatic Pressure Load

doi: 10.11858/gywlxb.2010.03.008

  • National Key Laboratory of Shock Wave and Detonation Physics, Institute of Fluid Physics, CAEP, Mianyang 621900, China

More Information
  • Corresponding author: BI Yan
  • Received Date: 01 Apr 2009
  • Rev Recd Date: 28 Oct 2009
  • Issue Publish Date: 15 Jun 2010
    Abstract
  • By measuring the sound velocity of single crystal MgO at high pressures and using the high pressure Brillouin scattering data, the pressures point by point (the oil-pressure points range from 15 MPa to 51 MPa with step of 2 MPa) in a wide pressure range in the cubic pressure cell under hydrostatic loading environment were calibrated. Furthermore, a novel pressure calibration technique for the large volume pressure cell was established. This new calibration method is more reliable than the traditional one which only depends on 2 or 3 phase transition points. As an example, the measured sound velocity in LY12 aluminum under this hydrostatic loading is in good agreement with published literature data, which further confirms that the novel pressure calibration method is feasible and reliable. Comparing the pressure in the high-pressure cell based on the solid-liquid hybrid assembly with that based on the all-solid one, it was found that the cell-pressure in the former is systematically lower. The analysis suggested that this phenomenon is due to the shear effect in all-solid assembly which makes the pressure scale much higher.

     

    • FullText(HTML)
  • loading
    • References(30)
  • Spetzler H. Equation of State of Polycrystalline and Single-Crystal MgO to 8 Kilobars and 800 K [J]. J Geophys Res, 1970, 75(11): 2073-2087.
    Xie H S, Zhang Y M, Xu H G, et al. A New Method of Measurement for Elastic Wave Velocities in Minerals and Rocks at High Temperature and High Pressure and Its Significance [J]. Science China Chemistry (Science in China Series B), 1993, 36(10): 1276-1280.
    Xu J A, Zhang Y, Hou W, et al. Measurements of Ultrasonic Wave Velocities at High Temperature and High Pressure for Window Glass Pyrophyllite and Kimberlite up to 1400 ℃ and 5. 5 GPa [J]. High Temperature-High Pressure, 1994, 26: 375-384.
    Liu Y G, Xie H S, Guo J, et al. A New Method for Experimental Determination of Compressional Velocities in Rocks and Minerals at High-Pressure [J]. Chin Phys Lett, 2000, 17(12): 924-926.
    Li B S, Jackson I, Gasparik T, et al. Elastic Wave Velocity Measurement in Multi-Anvil Apparatus to 10 GPa Using Ultrasonic Interferometry [J]. Phys Earth Planet Interiors, 1996, 98: 79-91.
    Spetzler H, Shen A, Chen G, et al. Ultrasonic Measurements in a Diamond Anvil Cell [J]. Phys Earth Planet Interiors, 1996, 98: 93-99.
    Wang Q S, Wang Z G, Bi Y. Design of the Sample Assembly for Ultrasonic Measurement at High Pressure and 300 K in Six-Side Anvil Cell [J]. Chinese Journal of High Pressure Physics, 2006, 20(3): 331-336. (in Chinese)
    王青松, 王志刚, 毕延. 六面顶压机上常温高压超声测量的样品组装设计 [J]. 高压物理学报, 2006, 20(3): 331-336.
    Decker D L, Zhao Y X. Dielectric and Polarization Measurements on BaTiO3 at High Pressures to the Tricritical Point [J]. Phys Rev B, 1989, 39(4): 2432-2438.
    Lu Z, Zhan X H, Cao D H, et al. A High Frequency Hydrostatic Pressure Dielectricity Measuring System Based on Cubic Anvil Apparatus [J]. Chinese Journal of High Pressure Physics, 2008, 22(1): 99-102. (in Chinese)
    陆中, 战晓红, 曹大呼, 等. 一套基于六面顶高压装置的静水压高频介电测试系统 [J]. 高压物理学报, 2008, 22(1): 99-102.
    Song M S, Yoneda A, Ito E. Solid-Liquid Hybrid Assembly for Ultrasonic Elasticity Measurements under Hydrostatic Conditions of up to 8 GPa in a Kawai-Type Multianvil Apparatus [J]. Rev Sci Instrum, 2005, 76(3): 033906.
    Song M S, Yoneda A, Ito E. Ultrasonic Measurements of Single-Crystal Gold under Hydrostatic Pressures up to 8 GPa in a Kawai-Type Multi-Anvil Apparatus [J]. Chinese Science Bulletin, 2007, 52(12): 1600-1606.
    Zhang D L, Wang L H. Design of Acquisition System with DSP Detecting Weak Signal [J]. Control Automation, 2005, 21(7): 83-85. (in Chinese)
    张冬玲, 王良红. 基于DSP的微弱信号检测采集系统设计 [J]. 微计算机信息, 2005, 21(7): 83-85.
    Piermarini G J, Block S, Barnett J D. Hydrostatic Limits in Liquids and Solids to 100 kbar [J]. J Appl Phys, 1973, 44: 5377-5382.
    Zhang Y, Cai L C, Bi Y. Programming Realization of Automatic Repeat Signals Acquisition Based on General Purpose Oscilloscope [J]. Chinese Journal of Scientific Instrument, 2008, 29(Supplement): 487-490. (in Chinese)
    张毅, 蔡灵仓, 毕延. 编程实现通用示波器自动重复采集 [J]. 仪器仪表学报, 2008, 29(增): 487-490.
    Zha C S, Mao H K, Hemley R J. Elasticity of MgO and a Primary Pressure Scale to 55 GPa [J]. Proc Natl Acad Sci, 2000, 97(25): 13494-13499.
    Karki B B, Stixrude L, Clark S J, et al. Structure and Elasticity of MgO at High Pressure [J]. American Mineralogist, 1997, 82(1-2): 51-60.
    Xie H S. Introduction to the Earth's Interior Materials Science [M]. Beijing: Science Press, 1997: 60. (in Chinese)
    谢鸿森. 地球深部物质科学导论 [M]. 北京: 科学出版社, 1997: 60.
    Li R, Ma H A, Yin B H, et al. Finite Element Analysis on Pressure-Transmitting Behavior of Pyrophyllite Block Based on ANSYS/LS-DYNA [J]. Journal of Jilin University (Engineering and Technology Edition), 2008, 38(2): 292-297. (in Chinese)
    李瑞, 马红安, 尹斌华, 等. 基于ANSYS/LS-DYNA的叶蜡石传压性能的有限元分析 [J]. 吉林大学学报(工学版), 2008, 38(2): 292-297.
    Decker D L, Petersen S, Debray D. Pressure-Induced Ferroelastic Phase Transition in Pb3(PO4)2: A Neutron-Diffraction Study [J]. Phys Rev B, 1979, 19(7): 3552-3555.
    Resel R, Oehzelt M, Shimizu K, et al. On the Phase-Transition in Anthracene Induced by High Pressure [J]. Solid State Commun, 2004, 129(2): 103-106.
    Zhang T, Bi Y, Zhao M G. Ultrasonic Measurement and Isothermal Equation of State for LY12Al under Static Pressures [J]. Chinese Journal of High Pressure Physics, 2005, 19(1): 35-40. (in Chinese)
    张婷, 毕延, 赵敏光. 静高压加载下LY12铝的超声测量与等温状态方程 [J]. 高压物理学报, 2005, 19(1): 35-40.
    Zhang T. Ultrasonic Measurements and Isothermal Equation of State for Three fcc Metals under Static Pressures [D]. Chengdu: Sichuan Normal University, 2004. (in Chinese)
    张婷. 静高压加载下几种面心立方金属的超声测量与等温物态方程研究 [D]. 成都: 四川师范大学, 2004.
    • Relative Articles
    • Supplements(0)
    • Cited By
  • 加载中

Catalog

    通讯作者: 陈斌, bchen63@163.com
    • 1. 

      沈阳化工大学材料科学与工程学院 沈阳 110142

    1. 本站搜索
    2. 百度学术搜索
    3. 万方数据库搜索
    4. CNKI搜索
    Get Citation
    PDF
    XML

    Article Metrics

    Article views(7812) PDF downloads(818) Cited by()
    Proportional views
    Related
    

    Website Copyright© Editorial Office of Chinese Journal of High Pressure Physics

    Tel:0816-2490042 E-mail:gaoya@caep.cn

    Shu ICP, 11011126 -2

    Supported by: Beijing Renhe Information Technology Co. Ltd support: info@rhhz.net  

    /

    DownLoad:  Full-Size Img  PowerPoint
    Return
    Return