knowledge of professional and technical personnel Notice on the organization of advanced research class on high-pressure science and new materials of engineering
Volume 32 Issue 2
Jan 2018
Turn off MathJax
Article Contents
Chinese Journal of High Pressure Physics  > 2018  >  32(2): 023302.
LU Jingrui, KOU Zili, LIU Teng, ZHANG Leilei, DING Wei, ZHANG Qiang, WANG Qiang, YANG Ming, GONG Hongxia, HE Duanwei. Sub-Micron Polycrystalline Diamond Synthesis under High Temperature and High Pressure[J]. Chinese Journal of High Pressure Physics, 2018, 32(2): 023302. doi: 10.11858/gywlxb.20170574
Citation: LU Jingrui, KOU Zili, LIU Teng, ZHANG Leilei, DING Wei, ZHANG Qiang, WANG Qiang, YANG Ming, GONG Hongxia, HE Duanwei. Sub-Micron Polycrystalline Diamond Synthesis under High Temperature and High Pressure[J]. Chinese Journal of High Pressure Physics, 2018, 32(2): 023302. doi: 10.11858/gywlxb.20170574
shu

Sub-Micron Polycrystalline Diamond Synthesis under High Temperature and High Pressure

doi: 10.11858/gywlxb.20170574

  • Institute of Atomic and Molecular Physics, Sichuan University, Chengdu 610065, China

  • Received Date: 03 May 2017
  • Rev Recd Date: 09 May 2017
    Abstract
  • Due to its wide range of applications as a superhard material, polycrystalline diamond (PCD) has been used in oil-and gas-drilling, tool cutting, making of wear-resistant parts.At present, the average size of industrial synthetic PCD is above the micron dimension, but synthesizing the PCD with a size below the micron dimension remains a tough challenge.In this work, we succeeded synthesizing sub-micron polycrystalline diamond under high temperature and high pressure using the infiltrating technique.The samples were characterized by X-ray diffraction (XRD), scanning electron microscope (SEM), electron backscatter diffraction (EBSD), energy dispersive spectrometer (EDS) and hardness test.These results show that the hardness of the PCD thus synthesized is 57.0GPa under 5.5GPa and 1500℃ when the hold time of temperature is 15min; that the Co can disperse uniformly in PCD as a round hole used the bi-layered assembly so that the PCD demonstrates uniform and excellent performance; and that it is found from its sintering process that the temperature and holding time play an important role in its synthetic process.

     

    • FullText(HTML)
  • loading
    • References(22)
  • [1]
    KANER R B, GILMAN J J, TOLBERT S H.Designing superhard materials[J]. Science, 2005, 308(5726):1268-1269. doi: 10.1126/science.1109830
    [2]
    HUANG Q, YU D L, XU B, et al.Nanotwinned diamond with unprecedented hardness and stability[J]. Nature, 2014, 510(7504):250. doi: 10.1038/nature13381
    [3]
    ZHAO Y, HE D W, DAEMEN L L, et al.Superhard B-C-N materials synthesized in nanostructured bulks[J]. Journal of Materials Research, 2002, 17(12):3139-3145. doi: 10.1557/JMR.2002.0454
    [4]
    IRIFUNE T, KURIO A, SAKAMOTO S, et al.Materials:ultrahard polycrystalline diamond from graphite[J]. Nature, 2003, 421(6923):599-600.
    [5]
    CHUNG H Y, WEINBERGER M B, LEVINE J B, et al.Synthesis of ultra-incompressible superhard rhenium diboride at ambient pressure[J]. Science, 2007, 316(5823):436-439. doi: 10.1126/science.1139322
    [6]
    DUBROVINSKAIA N, SOLOZHENKO V L, MIYAJIMA N, et al.Superhard nanocomposite of dense polymorphs of boron nitride:noncarbon material has reached diamond hardness[J]. Applied Physics Letters, 2007, 90(10):101912. doi: 10.1063/1.2711277
    [7]
    QIN J Q, HE D W, WANG J H, et al.Is rhenium diboride a superhard material?[J]. Advanced Materials, 2010, 20(24):4780-4783.
    [8]
    TIAN Y J, XU B, YU D L, et al.Ultrahard nanotwinned cubic boron nitride[J]. Nature, 2013, 493(7432):385-388. doi: 10.1038/nature11728
    [9]
    TANG H, WANG M Z, HE D W, et al.Synthesis of nano-polycrystalline diamond in proximity to industrial conditions[J]. Carbon, 2016, 108:1-6. doi: 10.1016/j.carbon.2016.07.004
    [10]
    BUNDY F P, HALL H T, STRONG H M, et al.Man-made diamonds[J]. Nature, 1955, 176(4471):51-55. doi: 10.1038/176051a0
    [11]
    SKURY A L D, BOBROVNITCHⅡ G S, MONTEIRO S N.The graphitization process and the synthesis of diamonds from a C-Ni-Mn system[J]. Carbon, 2004, 42(12/13):2369-2373.
    [12]
    HONG S M, AKAISHI M, KANDA H, et al.Dissolution behaviour of fine particles of diamond under high pressure sintering conditions[J]. Journal of Materials Science Letters, 1991, 10(3):164-166. doi: 10.1007/BF02352837
    [13]
    YAO B, WANG A M, DING B Z, et al.Study on structure of a new binding phase in polycrystalline diamond[J]. Journal of Materials Science Letters, 1995, 14(13):931-933. doi: 10.1007/BF02427468
    [14]
    HONG S M, AKAISHI M, KANDA H, et al.Behaviour of cobalt infiltration and abnormal grain growth during sintering of diamond on cobalt substrate[J]. Journal of Materials Science, 1988, 23(11):3821-3826. doi: 10.1007/BF01106798
    [15]
    HALL H T.Sintered diamond:a synthetic carbonado[J]. Science, 1970, 169(3948):868-869. doi: 10.1126/science.169.3948.868
    [16]
    KATZMAN H, LIBBY W F.Sintered diamond compacts with a cobalt binder[J]. Science, 1971, 172(3988):1132-1134. doi: 10.1126/science.172.3988.1132
    [17]
    WILKS J, WILKS E.Properties and applications of diamond[M]. Oxford:Butterworth-Heinemann, 1991.
    [18]
    AKAISHI M, OHSAWA T, YAMAOKA S.Synthesis of fine-grained polycrystalline diamond compact and its microstructure[J]. Journal of the American Ceramic Society, 1991, 74(1):5-10. doi: 10.1111/jace.1991.74.issue-1
    [19]
    BOVENKERK H P, KIBLER G M. Diamond and cubic boron nitride abrasive compacts using size selective abrasive particle layers: US 4311490 A[P]. 1982-01-19.
    [20]
    ZHANG Y, KOU Z, LI Y, et al.High pressure and high temperature sintering of fine-grained PCD using bi-layered assembly[J]. High Pressure Research, 2009, 29(2):325-334. doi: 10.1080/08957950802593774
    [21]
    XU C, HE D W, WANG H K, et al.Nano-polycrystalline diamond formation under ultra-high pressure[J]. International Journal of Refractory Metals & Hard Materials, 2013, 36(1):232-237. https://www.sciencedirect.com/science/article/pii/S0263436812001710
    [22]
    洪时明, 罗湘捷, 陈叔鑫, 等.D─D结合型金刚石聚晶的高压合成研究[J].高压物理学报, 1990, 4(2):105-113. http://www.gywlxb.cn/CN/abstract/abstract1228.shtml

    HONG S M, LUO X J, CHEN S X, et al.Experimental on sintering diamond with direct bonding between diamond particles[J]. Chinese Journal of High Pressure Physics, 1990, 4(2):105-113. http://www.gywlxb.cn/CN/abstract/abstract1228.shtml
    • Relative Articles
    • Supplements(0)
    • Cited By
  • 加载中

Catalog

    通讯作者: 陈斌, bchen63@163.com
    • 1. 

      沈阳化工大学材料科学与工程学院 沈阳 110142

    1. 本站搜索
    2. 百度学术搜索
    3. 万方数据库搜索
    4. CNKI搜索

    Figures(10)  / Tables(2)

    Get Citation
    PDF
    XML

    Article Metrics

    Article views(7450) PDF downloads(318) Cited by()
    Proportional views
    Related

    Copyright©《高压物理学报》编辑部

    Tel:0816-2490042 E-mail:gaoya@caep.cn

    Shu ICP, 11011126 -2

    Supported by: Beijing Renhe Information Technology Co. Ltd support: info@rhhz.net  

    /

    DownLoad:  Full-Size Img  PowerPoint
    Return
    Return