knowledge of professional and technical personnel Notice on the organization of advanced research class on high-pressure science and new materials of engineering
Volume 28 Issue 3
Jun 2015
Turn off MathJax
Article Contents
Chinese Journal of High Pressure Physics  > 2014  >  28(3): 319-323.
HAN Zhi-Wei, XIE Li-Feng, DENG Ji-Ping, NI Ou-Qi, XIE Yi-Chao, CHEN Ji-Yang. Detonation Synthesis and Characterization of Nano-Ceria with Emulsion Explosives[J]. Chinese Journal of High Pressure Physics, 2014, 28(3): 319-323. doi: 10.11858/gywlxb.2014.03.009
Citation: HAN Zhi-Wei, XIE Li-Feng, DENG Ji-Ping, NI Ou-Qi, XIE Yi-Chao, CHEN Ji-Yang. Detonation Synthesis and Characterization of Nano-Ceria with Emulsion Explosives[J]. Chinese Journal of High Pressure Physics, 2014, 28(3): 319-323. doi: 10.11858/gywlxb.2014.03.009
shu

Detonation Synthesis and Characterization of Nano-Ceria with Emulsion Explosives

doi: 10.11858/gywlxb.2014.03.009

  • School of Chemical Engineering, NUST, Nanjing 210094, China

  • Received Date: 16 May 2012
  • Rev Recd Date: 27 Jun 2012
    Abstract
  • In order to synthesize nano-ceria by detonation method, 5 kinds of emulsion explosives in which Ce(NO3)3·6H2O acted as main oxidant were designed and prepared.Considering the effects of the content of Ce(NO3)3 on the detonation velocity of emulsion explosives and the yield of nano-ceria, the formulas of emulsion explosives for preparing nano-ceria were screened.Nano-ceria was synthesized by initiating the emulsion explosive in explosion vessel.The as-synthesized products were characterized by XRD and TEM.The result from XRD test indicates that the nano-ceria belongs to cubic phase.The mean size of ceria grain is 74 nm based on the calculation result according to Scherrer equation.The result from TEM test presents that the as-synthesized ceria particles are spherical by appearance, they have well dispersion and the size was uniform.According to TEM test result, the mean diameter of ceria particles is about 70 nm, which coincides with the calculation result perfectly.

     

    • FullText(HTML)
  • loading
    • References(12)
  • [1]
    Yang J C, Kim H J, Kim T. Study of polishing characteristics of monodisperse ceria abrasive in chemical mechanical planarization[J]. J Electrochem Soc, 2010, 157(3): 235-240. doi: 10.1149/1.3273079
    [2]
    Moure A, Castro A, Martinez I, et al. Synthesis, sintering and ionic conductivity of scandia-doped ceria ceramic materials obtained by different procedures[J]. Ceram Int, 2012, 38(7): 5907-5914. doi: 10.1016/j.ceramint.2012.04.041
    [3]
    Wu X D, Liang Q, Weng D, et al. The catalytic activity of CuO-CeO2 mixed oxides for diesel soot oxidation with a NO/O2 mixture[J]. Catal Commun, 2007, 8(12): 2110-2114. doi: 10.1016/j.catcom.2007.04.023
    [4]
    Chen Y, Chen F L, Wang W D, et al. Sm0.2(Ce1-xTix)0.8O1.9 modified Ni-yttria-stabilized zirconia anode for direct methane fuel cell[J]. J Power Sources, 2011, 196(11): 4987-4991. doi: 10.1016/j.jpowsour.2011.01.062
    [5]
    Truffaulta L, Ta M T, Devers T, et al. Application of nanostructured Ca doped CeO2 for ultraviolet filtration[J]. Mater Res B, 2010, 45(5): 527-535. doi: 10.1016/j.materresbull.2010.02.008
    [6]
    Feng X D, Sayle D C, Wang Z L, et al. Converting ceria polyhedral nanoparticles into single-crystal nanospheres[J]. Science, 2006, 312(5779): 1504-1508. doi: 10.1126/science.1125767
    [7]
    Chiu J B, Yu C C, Shen S H. Application of soft landing to the process control of chemical mechanical polishing[J]. Microel Eng, 2003, 65(3): 345-356. doi: 10.1016/S0167-9317(02)01024-9
    [8]
    Chen P W, Ding Y S, Chen Q, et al. Spherical nanometer-sized diamond obtained from detonation[J]. Diam Relat, 2009, 9(9/10): 1722-1725. http://www.sciencedirect.com/science/article/pii/S092596350000306X
    [9]
    欧阳欣, 闫鸿浩, 刘津开, 等.纳米二氧化钛粉体的气相爆轰制备[J].高压物理学报, 2007, 21(4): 379-382. http://www.cqvip.com/Main/Detail.aspx?id=26403264

    Ouyang X, Yan H H, Liu J K, et al. Nano-titanium dioxide synthesis using gaseous detonation[J]. Chinese Journal of High Pressure Physics, 2007, 21(4): 379-382. (in Chinese) http://www.cqvip.com/Main/Detail.aspx?id=26403264
    [10]
    杜云艳, 李晓杰, 王小红, 等.硝酸铈爆轰制备球形纳米CeO2颗粒[J].爆炸与冲击, 2009, 29(1): 41-44.

    Du Y Y, Li X J, Wang X H, et al. Preparation of nano-sized CeO2 particles utilizing Ce(NO3)3·6H2O by detonation[J]. Explosion and Shock Waves, 2009, 29(1): 41-44. (in Chinese)
    [11]
    汪旭光.乳化炸药[M].第2版.北京: 冶金工业出版社, 2008: 181-185.

    Wang X G. Emulsion Explosives[M]. 2nd Ed. Beijing: Metallurgical Industry Press, 2008: 181-185. (in Chinese)
    [12]
    Courant R, Friedrichs K O. Supersonic Flow and Shock Waves[M]. New York: Springer, 1991: 211-214.
    • Relative Articles
    • Supplements(0)
    • Cited By
  • 加载中

Catalog

    通讯作者: 陈斌, bchen63@163.com
    • 1. 

      沈阳化工大学材料科学与工程学院 沈阳 110142

    1. 本站搜索
    2. 百度学术搜索
    3. 万方数据库搜索
    4. CNKI搜索

    Figures(6)

    Get Citation
    PDF
    XML

    Article Metrics

    Article views(7162) PDF downloads(277) Cited by()
    Proportional views
    Related

    Copyright©《高压物理学报》编辑部

    Tel:0816-2490042 E-mail:gaoya@caep.cn

    Shu ICP, 11011126 -2

    Supported by: Beijing Renhe Information Technology Co. Ltd support: info@rhhz.net  

    /

    DownLoad:  Full-Size Img  PowerPoint
    Return
    Return