knowledge of professional and technical personnel Notice on the organization of advanced research class on high-pressure science and new materials of engineering
Volume 28 Issue 3
Jun 2015
Turn off MathJax
Article Contents
Chinese Journal of High Pressure Physics  > 2014  >  28(3): 257-261.
FAN Da-Wei, XU Jin-Gui, WEI Shu-Yi, CHEN Zhi-Qiang, XIE Hong-Sen. In-Situ High-Pressure Synchrotron X-Ray Diffraction of Natural Epidote[J]. Chinese Journal of High Pressure Physics, 2014, 28(3): 257-261. doi: 10.11858/gywlxb.2014.03.001
Citation: FAN Da-Wei, XU Jin-Gui, WEI Shu-Yi, CHEN Zhi-Qiang, XIE Hong-Sen. In-Situ High-Pressure Synchrotron X-Ray Diffraction of Natural Epidote[J]. Chinese Journal of High Pressure Physics, 2014, 28(3): 257-261. doi: 10.11858/gywlxb.2014.03.001
shu

In-Situ High-Pressure Synchrotron X-Ray Diffraction of Natural Epidote

doi: 10.11858/gywlxb.2014.03.001
  • 1.

    Laboratory for High Temperature & High Pressure Study of the Earth's Interior of Institute of Geochemistry, Chinese Academy of Science, Guiyang 550002, China

  • 2.

    University of Chinese Academy of Sciences, Beijing 100049, China

  • 3.

    Department of Geoscience, Stony Brook University, New York 11794, USA

  • Received Date: 28 Oct 2012
  • Rev Recd Date: 06 Jan 2013
    Abstract
  • In situ angle dispersive X-ray diffraction measurements for a natural epidote were performed with diamond anvil cell instrument and synchrotron radiation at NSLS (National Synchrotron Light Source).The maximal pressure in the experiment was 9.16 GPa.At experimental pressures, no evidence of phase transition of the epidote was observed.A fit to the third-order Birch-Murnaghan equation of state yielded an isothermal bulk modulus of 116(7) GPa and its pressure derivative of 7.8(8).The isothermal bulk modulus of epidote is determined to be 132(4) GPa, assuming that its first pressure derivative is 4.Furthermore, we confirm that the linear compressibilities along a, b, and c directions of epidote are elastically anisotropic.Consequently, it can be concluded that the compressibility of epidote under high pressures has been accurately constrained.

     

    • FullText(HTML)
  • loading
    • References(12)
  • [1]
    潘兆橹, 赵爱醒, 潘铁虹.结晶学及矿物学[M].北京: 地质出版社, 1994: 28-30.

    Pan Z L, Zhao A X, Pan T H. Crystallography and Mineralogy[M]. Beijing: Geology Press, 1994: 28-30. (in Chinese)
    [2]
    翟伟, 孙晓明, 梁金龙, 等.青龙山超高压变质榴辉岩绿帘石化学成分与流体包裹体特征[J].岩石学报, 2006, 22(7): 2029-2038. http://d.wanfangdata.com.cn/Periodical/ysxb98200607030

    Zhai W, Sun X M, Liang J L, et al. Chemical compositions and fluid inclusions of epidotes in Qinglongshan ultrahigh pressure metamorphic eclogite north Jiangsu province, China[J]. Acta Petrologica Sinica, 2006, 22(7): 2029-2038. (in Chinese) http://d.wanfangdata.com.cn/Periodical/ysxb98200607030
    [3]
    Holland T J B, Redfern S A T, Pawley A R. Volume behavior of hydrous minerals at high pressure and temperature: Ⅱ. Compressibilities of lawsonite, zoisite, clinozoisite, and epidote[J]. Am Mineral, 1996, 81(3/4): 341-348. http://www.degruyter.com/view/j/ammin.1996.81.issue-3-4/am-1996-3-407/am-1996-3-407.xml
    [4]
    Qin S, Wu X, Liu J, et al. Compressibility of epidote up to 20 GPa at 298 K[J]. Chin Phys Lett, 2003, 20(7): 1172-1174. doi: 10.1088/0256-307X/20/7/358
    [5]
    Gatta G D, Merlini M, Lee Y, et al. Behavior of epidote at high pressure and high temperature: A powder diffraction study up to 10 GPa and 1200 K[J]. Phys Chem Miner, 2011, 38(6): 419-428. doi: 10.1007/s00269-010-0415-y
    [6]
    谢超, 杜建国, 李营, 等.在200 ℃和0.95-7.70 GPa下天然斜绿泥石的拉曼光谱特征[J].光谱学与光谱分析, 2010, 30(12): 3232-3235. http://www.cnki.com.cn/Article/CJFDTotal-GUAN201012018.htm

    Xie C, Du J G, Li Y, et al. Characteristics of Raman spectra of natural clinochlore at 200 ℃ and 0.95-7.70 GPa[J]. Spectroscopy and Spectral Analysis, 2010, 30(12): 3232-3235. (in Chinese) http://www.cnki.com.cn/Article/CJFDTotal-GUAN201012018.htm
    [7]
    秦善, 刘景, 李海建, 等.绿柱石的原位高压X射线研究[J].高压物理学报, 2008, 22(1): 1-5. http://www.cqvip.com/Main/Detail.aspx?id=27084718

    Qin S, Liu J, Li H J, et al. In-situ high-pressure X-ray diffraction of natural beryl[J]. Chinese Journal of High Pressure Physics, 2008, 22(1): 1-5. (in Chinese) http://www.cqvip.com/Main/Detail.aspx?id=27084718
    [8]
    Mao H K, Xu J, Bell P M. Calibration of the ruby pressure gauge to 800 kbar under quasi-hydrostatic conditions[J]. J Geophys Res, 1986, 91(B5): 4673-4676. doi: 10.1029/JB091iB05p04673
    [9]
    Holland T J B, Redfern S A T. Unit cell refinement from powder diffraction data: The use of regression diagnostics[J]. Mineral Mag, 1997, 61(1): 65-77. http://www.degruyter.com/view/j/minmag.1997.61.issue-1/minmag.1997.061.404.07/minmag.1997.061.404.07.xml?format=INT
    [10]
    Birch F. Finite elastic strain of cubic crystals[J]. Phys Rev, 1947, 71(11): 809-824. doi: 10.1103/PhysRev.71.809
    [11]
    Angel R J, Bujak M, Zhao J, et al. Effective hydrostatic limits of pressure media for high-pressure crystallographic studies[J]. J Appl Crystallogr, 2007, 40(1): 26-32. doi: 10.1107/S0021889806045523
    [12]
    Fan D W, Ma M N, Yang J J, et al. In situ high pressure synchrotron X-ray diffraction study of clinozoisite[J]. Chin Phys Lett, 2011, 28(12): 126103. doi: 10.1088/0256-307X/28/12/126103
    • Relative Articles
    • Supplements(0)
    • Cited By
  • 加载中

Catalog

    通讯作者: 陈斌, bchen63@163.com
    • 1. 

      沈阳化工大学材料科学与工程学院 沈阳 110142

    1. 本站搜索
    2. 百度学术搜索
    3. 万方数据库搜索
    4. CNKI搜索

    Figures(4)  / Tables(2)

    Get Citation
    PDF
    XML

    Article Metrics

    Article views(6667) PDF downloads(287) Cited by()
    Proportional views
    Related

    Copyright©《高压物理学报》编辑部

    Tel:0816-2490042 E-mail:gaoya@caep.cn

    Shu ICP, 11011126 -2

    Supported by: Beijing Renhe Information Technology Co. Ltd support: info@rhhz.net  

    /

    DownLoad:  Full-Size Img  PowerPoint
    Return
    Return