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Chinese Journal of High Pressure Physics  > 2006  >  20(2): 220-224 .
JIN Bo, PENG Ru-Fang, SHU Yuan-Jie, ZHONG Fa-Chun, CHU Shi-Jin. Study on the Synthesis of New Energetic Fullerene Derivative[J]. Chinese Journal of High Pressure Physics, 2006, 20(2): 220-224 . doi: 10.11858/gywlxb.2006.02.019
Citation: JIN Bo, PENG Ru-Fang, SHU Yuan-Jie, ZHONG Fa-Chun, CHU Shi-Jin. Study on the Synthesis of New Energetic Fullerene Derivative[J]. Chinese Journal of High Pressure Physics, 2006, 20(2): 220-224 . doi: 10.11858/gywlxb.2006.02.019
shu

Study on the Synthesis of New Energetic Fullerene Derivative

doi: 10.11858/gywlxb.2006.02.019
  • 1.

    School of Material Science and Engineering, Southwest University of Science and Technology, Mianyang 621010, China;

  • 2.

    Institute of Chemical Materials, CAEP, Mianyang 621900, China

More Information
  • Corresponding author: PENG Ru-Fang
  • Received Date: 10 Aug 2005
  • Rev Recd Date: 20 Oct 2005
  • Publish Date: 05 Jun 2006
    Abstract
  • A new fullerene derivative 1 which contains energy-producing groups was prepared by the Prato reaction, and the reaction conditions affecting the yield of product 1 were investigated. The optimized reaction conditions which afforded 65.8% (based on consumed C60) of product 1 are: molar ratio of C60, 2, 4-dinitrobenzaldehyde and N-methylglycine 1∶2∶6, reaction temperature 95 ℃, reaction time 40 h. The structure of product 1 was characterized by UV-vis, FT-IR, 1H NMR and MS. Further study on the property and application of 1 is under way.

     

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