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Chinese Journal of High Pressure Physics  > 1995  >  9(2): 89-95 .
LIU Xiao-Yang, ZHAO Xu-Dong, HOU Wei-Min, SU Wen-Hui. Synthesis and Characterization of Boron Suboxide B7O under High Pressure and High Temperature[J]. Chinese Journal of High Pressure Physics, 1995, 9(2): 89-95 . doi: 10.11858/gywlxb.1995.02.002
Citation: LIU Xiao-Yang, ZHAO Xu-Dong, HOU Wei-Min, SU Wen-Hui. Synthesis and Characterization of Boron Suboxide B7O under High Pressure and High Temperature[J]. Chinese Journal of High Pressure Physics, 1995, 9(2): 89-95 . doi: 10.11858/gywlxb.1995.02.002
shu

Synthesis and Characterization of Boron Suboxide B7O under High Pressure and High Temperature

doi: 10.11858/gywlxb.1995.02.002
  • 1.

    Physics Departement, Jilin University, Changchun 130023, China;

  • 2.

    International Center for Materials Physicss, Academia Sinica, Shenyang 110015, China

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  • Corresponding author: LIU Xiao-Yang
  • Received Date: 01 Feb 1994
  • Rev Recd Date: 31 Mar 1994
  • Publish Date: 05 Jun 1995
    Abstract
  • The red-brown boron-rich solid B7O has been synthesized by means of oxidation of boron with zinc oxide under conditions of 3.5 GPa and 1 200 ℃ for 30 min. The product after leached in hydrochroric acid has been characterized by XRD, XPS, IR, SIMS and chemical analysis. The results of SIMS and chemical analysis show that the chemical formula is B7O. The results of X-ray powder diffraction indicates that the crystal structure of the sample can be classified as hexagonal symmetry with lattice constants of =0.543 5 nm and c=1.2415 nm.

     

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