Volume 27 Issue 5
Mar 2015
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WANG Hai-Kuo, HE Duan-Wei, XU Chao, GUAN Jun-Wei, WANG Wen-Dan, KOU Zi-Li, PENG Fang. Development of Large Volume-High Static Pressure Techniques Based on the Hinge-Type Cubic Presses[J]. Chinese Journal of High Pressure Physics, 2013, 27(5): 633-661. doi: 10.11858/gywlxb.2013.05.001
Citation: WANG Hai-Kuo, HE Duan-Wei, XU Chao, GUAN Jun-Wei, WANG Wen-Dan, KOU Zi-Li, PENG Fang. Development of Large Volume-High Static Pressure Techniques Based on the Hinge-Type Cubic Presses[J]. Chinese Journal of High Pressure Physics, 2013, 27(5): 633-661. doi: 10.11858/gywlxb.2013.05.001

Development of Large Volume-High Static Pressure Techniques Based on the Hinge-Type Cubic Presses

doi: 10.11858/gywlxb.2013.05.001
  • Received Date: 27 Aug 2013
  • Rev Recd Date: 24 Sep 2013
  • Publish Date: 15 Oct 2013
  • The large volume press (LVP) becomes more and more popular with the scientific and technological workers in the high pressure area, because it could generate relatively higher pressure, provide better hydrostatic pressure and could be utilized in conjunction with in situ X-ray diffraction, neutron diffraction and ultrasonic measurement. There have been generally two LVP techniques to generate high-pressure: the double-anvil apparatus and the multi-anvil apparatus (MAA). Hinge-type cubic presses, as the main apparatus in china, have been widely used in the fields of both scientific research and diamond industry. However, for a long time past, the maximum pressure using the conventional one-stage anvil system for hinge-type cubic press is about 6 GPa, and the techniques about two-stage apparatus (octahedral press) that could generate pressure exceed 20 GPa is blank in our country. To a certain extent, the backwardness of the LVP technology in china restricts the development of high pressure science and related subjects. In recent years, we designed two kinds of one-stage high pressure apparatus and the two-stage apparatus based on hinge-type cubic-anvil press, the one-stage high pressure apparatus and the two-stage apparatus using cemented carbide as anvils could generate pressures up to about 9 GPa and 20 GPa respectively. This article mainly reviews the mechanics structure, design of cell assembly, pressure and temperature calibration, design and preparation of the sintered diamond anvils and pressure calibration to 35 GPa using sintered diamond as two-stage anvils about the one-stage high pressure apparatus and the two-stage apparatus designed in our laboratory.

     

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