上海同步辐射光源高压相关线站概述

杨科 蒋升 闫帅 周春银 李爱国

杨科, 蒋升, 闫帅, 周春银, 李爱国. 上海同步辐射光源高压相关线站概述[J]. 高压物理学报, 2020, 34(5): 050102. doi: 10.11858/gywlxb.20200584
引用本文: 杨科, 蒋升, 闫帅, 周春银, 李爱国. 上海同步辐射光源高压相关线站概述[J]. 高压物理学报, 2020, 34(5): 050102. doi: 10.11858/gywlxb.20200584
YANG Ke, JIANG Sheng, YAN Shuai, ZHOU Chunyin, LI Aiguo. Application of Shanghai Synchrotron Radiation Source in High Pressure Research[J]. Chinese Journal of High Pressure Physics, 2020, 34(5): 050102. doi: 10.11858/gywlxb.20200584
Citation: YANG Ke, JIANG Sheng, YAN Shuai, ZHOU Chunyin, LI Aiguo. Application of Shanghai Synchrotron Radiation Source in High Pressure Research[J]. Chinese Journal of High Pressure Physics, 2020, 34(5): 050102. doi: 10.11858/gywlxb.20200584

上海同步辐射光源高压相关线站概述

doi: 10.11858/gywlxb.20200584
详细信息
    作者简介:

    杨 科(1978-),男,博士,研究员,主要从事同步辐射实验技术研究. E-mail:yangke@zjlab.org.cn

  • 中图分类号: O434.19; O521.3

Application of Shanghai Synchrotron Radiation Source in High Pressure Research

  • 摘要: 同步辐射X射线与基于金刚石对顶砧(DAC)和大体积压机(LVP)的静高压技术的结合推动了高压科学的发展。上海同步辐射光源(SSRF)是性能指标达到世界一流的中能第三代同步辐射光源,其中的硬X射线微聚焦及应用光束线站(BL15U1)具备高通量、能量可调的单色微束X射线,空间分辨达到微米至亚微米量级,在开展DAC高压研究方面有相当大的优势。自2010年对从事高压科学研究的用户开放以来,国内外高压科学研究者综合利用BL15U1线站高压实验方法取得了一系列有影响力的成果。此外,在建的上海光源二期线站工程中的超硬多功能线站(BL12SW)中配备200 t和2 000 t大压机,将成为开展LVP原位高压实验的有力平台。为促进用户对SSRF高压研究相关线站的了解,更好地利用相关平台开展研究工作,并为后续线站建设和实验方法发展提出宝贵建议,本文对BL15U1和BL12SW线站的布局、性能指标、实验站主要设施以及相关实验方法等进行了较为完整的介绍。

     

  • 图  HXMF光束线布局

    Figure  1.  Schematic layout of HXMF beamline

    图  HXMF实验站布局

    Figure  2.  Schematic layout of HXMF experimental station

    图  HXMF实验站照片

    Figure  3.  Photo of HXMF experimental station

    图  红宝石荧光测压光路

    Figure  4.  Optical system for measuring ruby fluorescence

    图  Renishaw拉曼光谱仪

    Figure  5.  Renishaw Raman spectrometer

    图  便携式红宝石测压系统

    Figure  6.  Portable ruby high pressure calibration system

    图  HXMF实验站样品控制平台示意图

    Figure  7.  Schematic of sample stages of HXMF experimental station

    图  HXMF实验站六轴样品控制台

    Figure  8.  Six axis sample stages of HXMF experimental station

    图  样品架结构的爆炸视图

    Figure  9.  Explosion view of sample holder structure

    图  10  DAC高压装置

    Figure  10.  High pressure device of DAC

    图  11  二氧化铈的XRD谱(Mar165 CCD共有2048 × 2048个像素点,每个像素点尺寸为80 μm× 80 μm)

    Figure  11.  XRD pattern of CeO2 (Mar165 CCD has 2048 × 2048 pixels, the size of each pixel is 80 μm× 80 μm)

    图  12  HXMF实验系统的笛卡尔坐标系和旋转自由度

    Figure  12.  Cartesian coordinate system and rotational degrees of freedom of HXMF experimental system

    图  13  高压单晶衍射样品控制平台

    Figure  13.  Sample control platform for high pressure single crystal diffraction

    图  14  HXMF线站可分析的元素

    Figure  14.  Analyzable elements of HXMF beamline

    图  15  超硬多功能光束线布局

    Figure  15.  Schematic layout of super-hard multifunction beamline

    图  16  高压原位实验站实验方法

    Figure  16.  Experimental methods of in situ high pressure experimental station

    图  17  200 t压机示意图(图片来源:Max Voggenreiter)

    Figure  17.  Schematic diagram of 200 t LVP (Image source: Max Voggenreiter)

    图  18  2000 t压机示意图(图片来源:Max Voggenreiter)

    Figure  18.  Schematic diagram of 2000 t LVP (Image source:Max Voggenreiter)

    表  1  HXMF线站的主要指标

    Table  1.   Main parameters of HXMF beamline

    Light source typeEnergy/
    keV
    Energy resolution
    ($ {\text{Δ}}E/E$)
    Photon flux/[phs·s−1·$ {\text{μ}}{\rm{m}}$−2·
    (0.1%B.W.)−1]
    Beam size at sample/
    (μm × μm)
    Divergence at sample/
    (mrad × mrad)
    Undulator5−20 < 2 × 10−4
    Si (111)
    > 1012 < 2 × 2
    (K-B mirrors)
    < 2 (H) × 1.5 (V)
    (K-B mirrors)
    下载: 导出CSV

    表  2  超硬多功能线站的技术指标

    Table  2.   Technical specification of super-hard multifunction station

    Energy/keVEnergy resolution ($ {\text{Δ}}E/E$)Photon flux/(phs·s−1@100 keV@25 μrad)Spot size at sample/(mm×mm)
    30−150 < 9 × 10−32 × 10110.5 × 0.5(Focused mode);
    Max:100 (H) × 30 (V)
    (Non-focusing mode)
    下载: 导出CSV
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  • 收稿日期:  2020-07-03
  • 修回日期:  2020-08-04

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