Synchrotron Radiation X-Ray Diffraction Study on Mn3Zn0.8Ni0.2N under High Pressure
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摘要: 利用金刚石对顶压砧,对钙钛矿型金属锰化物Mn3Zn0.8Ni0.2N进行了原位高压同步辐射角散X射线衍射研究。研究表明,在0~29.9 GPa的压力区间内,样品没有发生结构相变,因而在该压力下样品的物性变化并非由结构相变所导致。卸压以后,样品的特征峰都回到了初始位置。通过Birch-Murnaghan方程,拟合得到了样品的体弹模量为86.5 GPa。Abstract: The structural stability of Mn3Zn0.8Ni0.2N was investigated up to 29.9 GPa by in situ angle dispersive X-ray diffraction using synchrotron radiation source and a diamond anvil cell. No structural phase transition was observed in the pressure range of 0-29.9 GPa. This result indicates that the changes in the physical properties of Mn3Zn0.8Ni0.2N under pressure are not induced by structural phase transition. Through fitting the Birch-Murnaghan equation, we obtain the bulk modulus B0= 86.5 GPa for Mn3Zn0.8Ni0.2N, assuming its first order derivative B0=4 at ambient pressure.
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Key words:
- anti-perovskite /
- high pressure /
- synchrotron X-ray diffraction /
- bulk modulus
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