静水压加载单晶MgO的超声测量与压力标定

张毅 毕延 蔡灵仓 徐济安

张毅, 毕延, 蔡灵仓, 徐济安. 静水压加载单晶MgO的超声测量与压力标定[J]. 高压物理学报, 2010, 24(3): 206-212 . doi: 10.11858/gywlxb.2010.03.008
引用本文: 张毅, 毕延, 蔡灵仓, 徐济安. 静水压加载单晶MgO的超声测量与压力标定[J]. 高压物理学报, 2010, 24(3): 206-212 . doi: 10.11858/gywlxb.2010.03.008
ZHANG Yi, BI Yan, CAI Ling-Cang, XU Ji-An. Ultrasonic Velocity Measurement and Pressure Calibration of Single Crystal MgO under Hydrostatic Pressure Load[J]. Chinese Journal of High Pressure Physics, 2010, 24(3): 206-212 . doi: 10.11858/gywlxb.2010.03.008
Citation: ZHANG Yi, BI Yan, CAI Ling-Cang, XU Ji-An. Ultrasonic Velocity Measurement and Pressure Calibration of Single Crystal MgO under Hydrostatic Pressure Load[J]. Chinese Journal of High Pressure Physics, 2010, 24(3): 206-212 . doi: 10.11858/gywlxb.2010.03.008

静水压加载单晶MgO的超声测量与压力标定

doi: 10.11858/gywlxb.2010.03.008
详细信息
    通讯作者:

    毕延

Ultrasonic Velocity Measurement and Pressure Calibration of Single Crystal MgO under Hydrostatic Pressure Load

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    Corresponding author: BI Yan
  • 摘要: 通过对单晶MgO的高压声速测量,结合高压Brillouin散射数据,对静水压加载条件下六面顶压机高压腔中的压力进行了多点系统标定(系统油压从15 MPa到51 MPa,间隔2 MPa),建立了新的大腔体压机超声测量和压力标定技术。相比传统的仅采用2~3个标定压力点的方法,该技术在统计上更加可靠。结合LY12铝的高压声速测量,进一步验证了该压力标定方法的合理性。与固体传压组装相比,固液混合传压组装在相同油压下的压力值系统偏低,分析认为这主要是由于固体传压介质中的剪切效应导致标定压力值系统偏高造成的。

     

  • Spetzler H. Equation of State of Polycrystalline and Single-Crystal MgO to 8 Kilobars and 800 K [J]. J Geophys Res, 1970, 75(11): 2073-2087.
    Xie H S, Zhang Y M, Xu H G, et al. A New Method of Measurement for Elastic Wave Velocities in Minerals and Rocks at High Temperature and High Pressure and Its Significance [J]. Science China Chemistry (Science in China Series B), 1993, 36(10): 1276-1280.
    Xu J A, Zhang Y, Hou W, et al. Measurements of Ultrasonic Wave Velocities at High Temperature and High Pressure for Window Glass Pyrophyllite and Kimberlite up to 1400 ℃ and 5. 5 GPa [J]. High Temperature-High Pressure, 1994, 26: 375-384.
    Liu Y G, Xie H S, Guo J, et al. A New Method for Experimental Determination of Compressional Velocities in Rocks and Minerals at High-Pressure [J]. Chin Phys Lett, 2000, 17(12): 924-926.
    Li B S, Jackson I, Gasparik T, et al. Elastic Wave Velocity Measurement in Multi-Anvil Apparatus to 10 GPa Using Ultrasonic Interferometry [J]. Phys Earth Planet Interiors, 1996, 98: 79-91.
    Spetzler H, Shen A, Chen G, et al. Ultrasonic Measurements in a Diamond Anvil Cell [J]. Phys Earth Planet Interiors, 1996, 98: 93-99.
    Wang Q S, Wang Z G, Bi Y. Design of the Sample Assembly for Ultrasonic Measurement at High Pressure and 300 K in Six-Side Anvil Cell [J]. Chinese Journal of High Pressure Physics, 2006, 20(3): 331-336. (in Chinese)
    王青松, 王志刚, 毕延. 六面顶压机上常温高压超声测量的样品组装设计 [J]. 高压物理学报, 2006, 20(3): 331-336.
    Decker D L, Zhao Y X. Dielectric and Polarization Measurements on BaTiO3 at High Pressures to the Tricritical Point [J]. Phys Rev B, 1989, 39(4): 2432-2438.
    Lu Z, Zhan X H, Cao D H, et al. A High Frequency Hydrostatic Pressure Dielectricity Measuring System Based on Cubic Anvil Apparatus [J]. Chinese Journal of High Pressure Physics, 2008, 22(1): 99-102. (in Chinese)
    陆中, 战晓红, 曹大呼, 等. 一套基于六面顶高压装置的静水压高频介电测试系统 [J]. 高压物理学报, 2008, 22(1): 99-102.
    Song M S, Yoneda A, Ito E. Solid-Liquid Hybrid Assembly for Ultrasonic Elasticity Measurements under Hydrostatic Conditions of up to 8 GPa in a Kawai-Type Multianvil Apparatus [J]. Rev Sci Instrum, 2005, 76(3): 033906.
    Song M S, Yoneda A, Ito E. Ultrasonic Measurements of Single-Crystal Gold under Hydrostatic Pressures up to 8 GPa in a Kawai-Type Multi-Anvil Apparatus [J]. Chinese Science Bulletin, 2007, 52(12): 1600-1606.
    Zhang D L, Wang L H. Design of Acquisition System with DSP Detecting Weak Signal [J]. Control Automation, 2005, 21(7): 83-85. (in Chinese)
    张冬玲, 王良红. 基于DSP的微弱信号检测采集系统设计 [J]. 微计算机信息, 2005, 21(7): 83-85.
    Piermarini G J, Block S, Barnett J D. Hydrostatic Limits in Liquids and Solids to 100 kbar [J]. J Appl Phys, 1973, 44: 5377-5382.
    Zhang Y, Cai L C, Bi Y. Programming Realization of Automatic Repeat Signals Acquisition Based on General Purpose Oscilloscope [J]. Chinese Journal of Scientific Instrument, 2008, 29(Supplement): 487-490. (in Chinese)
    张毅, 蔡灵仓, 毕延. 编程实现通用示波器自动重复采集 [J]. 仪器仪表学报, 2008, 29(增): 487-490.
    Zha C S, Mao H K, Hemley R J. Elasticity of MgO and a Primary Pressure Scale to 55 GPa [J]. Proc Natl Acad Sci, 2000, 97(25): 13494-13499.
    Karki B B, Stixrude L, Clark S J, et al. Structure and Elasticity of MgO at High Pressure [J]. American Mineralogist, 1997, 82(1-2): 51-60.
    Xie H S. Introduction to the Earth's Interior Materials Science [M]. Beijing: Science Press, 1997: 60. (in Chinese)
    谢鸿森. 地球深部物质科学导论 [M]. 北京: 科学出版社, 1997: 60.
    Li R, Ma H A, Yin B H, et al. Finite Element Analysis on Pressure-Transmitting Behavior of Pyrophyllite Block Based on ANSYS/LS-DYNA [J]. Journal of Jilin University (Engineering and Technology Edition), 2008, 38(2): 292-297. (in Chinese)
    李瑞, 马红安, 尹斌华, 等. 基于ANSYS/LS-DYNA的叶蜡石传压性能的有限元分析 [J]. 吉林大学学报(工学版), 2008, 38(2): 292-297.
    Decker D L, Petersen S, Debray D. Pressure-Induced Ferroelastic Phase Transition in Pb3(PO4)2: A Neutron-Diffraction Study [J]. Phys Rev B, 1979, 19(7): 3552-3555.
    Resel R, Oehzelt M, Shimizu K, et al. On the Phase-Transition in Anthracene Induced by High Pressure [J]. Solid State Commun, 2004, 129(2): 103-106.
    Zhang T, Bi Y, Zhao M G. Ultrasonic Measurement and Isothermal Equation of State for LY12Al under Static Pressures [J]. Chinese Journal of High Pressure Physics, 2005, 19(1): 35-40. (in Chinese)
    张婷, 毕延, 赵敏光. 静高压加载下LY12铝的超声测量与等温状态方程 [J]. 高压物理学报, 2005, 19(1): 35-40.
    Zhang T. Ultrasonic Measurements and Isothermal Equation of State for Three fcc Metals under Static Pressures [D]. Chengdu: Sichuan Normal University, 2004. (in Chinese)
    张婷. 静高压加载下几种面心立方金属的超声测量与等温物态方程研究 [D]. 成都: 四川师范大学, 2004.
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出版历程
  • 收稿日期:  2009-04-01
  • 修回日期:  2009-10-28
  • 发布日期:  2010-06-15

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