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摘要: 研究了经冲击波处理的羟基磷灰石粉末团聚体的活性及其烧结性能。X射线衍射(XRD)及扫描电镜(SEM)分析表明,冲击波对羟基磷灰石团聚体粉末具有明显的均化与细化作用,并产生了一定程度的晶格畸变,可促进羟基磷灰石陶瓷的烧结。粉体中储存的缺陷能在烧结过程中释放,使受冲击试样比未受冲击试样达到最大线收缩率时的温度降低70 ℃,羟基磷灰石陶瓷的强度和密度明显提高。Abstract: Hydroxyapatite (HA) is an effective material used in bone prostheses. The activating and sintering characteristics of hydroxyapatite agglomerate treated by shock wave were studied. Using XRD and SEM the grain size refinement, homogenization and lattice deformation were observed in shocked HA powders, which can promote sintering of HA ceramics. The extra energy stored in shocked powders will be released during sintering process. The temperature of maximum shrink rate of shocked sample is about 70 lower than that of unshocked one. The strength and density of HA ceramics from the shocked sample can be enhanced. HA ceramics with high strength used for artificial bone materials can be made with the shock-activating method.
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Key words:
- hydroxyapatite /
- shock-activating /
- sintering /
- biomedical ceramics
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